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Effect of Sodium Hydroxide on the Fast Synthesis of Superhydro-phobic Powder from Polymethylhydrosiloxane
ISSN: 2369 - 3355
Publisher: author
Effect of Sodium Hydroxide on the Fast Synthesis of Superhydro-phobic Powder from Polymethylhydrosiloxane
Indexed in
Technology and Engineering
ARTICLE-FACTOR
1.3
Article Basics Score: 3
Article Transparency Score: 3
Article Operation Score: 3
Article Articles Score: 3
Article Accessibility Score: 2
SUBMIT PAPER ASK QUESTION
International Category Code (ICC):
ICC-1802
Publisher: Lifescience Global Inc.
International Journal Address (IAA):
IAA.ZONE/2369108613355
eISSN
:
2369 - 3355
VALID
ISSN Validator
Abstract
The paper reports the role of sodium hydroxide in the synthesis of a superhydrophobic powder from polymethylhydrosiloxane (PMHS) in the presence of ethanol and water. The effects of other basic and acidic solutions as well as the absence of water were also investigated. PMHS exhibited rapid gelation (from 8 h to 2 h) by increasing the concentration of sodium hydroxide in the presence of ethanol and water. In contrast, gelation did not occur in the absence of sodium hydroxide or water or in the presence of acidic solutions. Delayed gelation (96 h to 120 h) occurred as a result of the introduction of dipotassium hydrogen phosphate trihydrate. Superhydrophobic powder was obtained by the evaporation of solvents from the gelated sol at 150 °C. The surface properties of the superhydrophobic powder were examined by scanning electron microscopy, high resolution transmission electron microscopy, N2 sorption isotherm, and X-ray diffraction. The...
